Research data supporting [Unveiling the role of boroxines in metal-free carbon-carbon homologations using diazo compounds and boronic acid]Claudio Bomio-Confaglia, Mikhail Kabeshov, Arthur Lit, Shing Hing Lau, J Ehlert, Claudio Battilocchio & Steven Ley
By means of computational and experimental mechanistic studies the fundamental role of boroxines in the reaction between diazo compounds and boronic acids was elucidated. Consequently, a selective metalfree carbon–carbon homologation of aryl and vinyl boroxines using TMSCHN2, giving access to TMSpinacol boronic ester products, was developed.
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